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- W2393020329 abstract "Objective To establish an HPLC method for the determination of icariin and tanshinoneⅡA in Jiliu Huaxiao Granules. Methods HPLC was carried out on a DiamonsilTM C18( 200 mm × 4.6 mm, 5 μm) column with acetonitrile- water as mobile phase for gradient elution. The detection wavelength was set at 270 nm. The injection volume was 10 μL at the flow rate of 1.0 mL/min. The temperature of column was set at 40 ℃. Results There was good linear relationship of icariin and tanshinoneⅡA in the range of 7.5 — 50 μg(r = 0.999 9) and 3 — 20 μg(r = 0.999 9), and the average recoveries were 100.2% and 100.1% with RSD values of 0.9% and 1.3%, respectively. Conclusion The method is simple to operate and reproducible, which can control the quality of Jiliu Huaxiao Granules effectively." @default.
- W2393020329 created "2016-06-24" @default.
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- W2393020329 date "2014-01-01" @default.
- W2393020329 modified "2023-09-26" @default.
- W2393020329 title "Determination of icariin and tanshinoneII_A in Jiliu Huaxiao Granules by HPLC" @default.
- W2393020329 hasPublicationYear "2014" @default.
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