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- W2393046050 abstract "By orthogonal experimental method,the effects of synthesis factors on the performances of lithium ion-sieve adsorbent MnO2 · 0.5H2O were studied.The mainly synthesis factors are hydrothermal temperature,n(Li)∶n(Mn),hydrothermal reaction time,calcination temperature and calcination time.The results show that the factors affect the absorption capacity of the lithium ionsieve,but the loss ratio of dissolved Mn has no significant change.The optimal conditions for preparation of lithium ion-sieve have determined such as hydrothermal temperature of 230 ℃,lithiummanganese molar ratio of 5∶1,reaction time of 13 h,calcination temperature of 450℃and calcination time of 6h.Ten cycles absorption/desorption experiments using the lithium ion-sieve prepared under optimal conditions were performed.The absorption capacity in first absorption process is 37.18mg/g.The absorption capacity remain 36.11mg/g after ten consecutive cycles of absorption desorption.The loss ratio of dissolved Mn is lower in these processes.The samples,which before and after absorption desorption process,were characterized by XRD.The results show that the samples always maintain Li1.6Mn1.6O4 spinel structure." @default.
- W2393046050 created "2016-06-24" @default.
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- W2393046050 date "2014-01-01" @default.
- W2393046050 modified "2023-09-26" @default.
- W2393046050 title "Effect of Synthesis Conditions on Properties of MnO_2·0.5H_2O Lithium Ion-Sieve Adsorbent" @default.
- W2393046050 hasPublicationYear "2014" @default.
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