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- W2393252618 abstract "p-Fluorobenzoylchloride was synthesized with p-fluorotoluene by photochlorination,hydrolysis and vacuum distillation.In the presence of visible light and side-reaction inhibitor,p-fluorotoluene reacted with chlorine at 125-145 ℃,the yield of p-fluorobenzotrichloride was 94.8%;p-fluorotoluene reacted with water at 120 ℃,the mole ratio of water to p-fluorobenzotrichloride was 0.98∶1,the yield of p-fluorobenzoyl chloride was 91.5%,the total yield of p-fluorobenzoyl chloride was 86.7%.The structure of target product was identified by IR,MS and 1H NMR." @default.
- W2393252618 created "2016-06-24" @default.
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- W2393252618 date "2012-01-01" @default.
- W2393252618 modified "2023-09-24" @default.
- W2393252618 title "Synthesis of p-Fluorobenzoyl Chloride" @default.
- W2393252618 hasPublicationYear "2012" @default.
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