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- W2393392248 abstract "Hybrid particles of hexamethylene diisocyanate/SiO2(HDI/SiO2) and hexamethyldisilazane/hexamethylene diisocyanate/SiO2(HMDS/HDI/SiO2) were fabricated by mechanochemical method based on high energy ball milling(HEBM).The prepared hybrid particles were characterized by Fourier transform infrared spectrometry(FT-IR),static contact angle(CA),titration method,thermal analysis(TGA),transmission electron microscopy(TEM),and particle size distribution.The results showed that the grafting density of HDI on silica particles increased with the increasing of the mass ratio of HDI to silica particles,and the saturated grafting density was 2.14 HDI/nm2 from titration results.HDI together with HDMS were chemically anchored to the surface of nano-SiO2.The grafting density of HDI was as high as 2.33 HDI/nm2,while the grafting density of HDMS was 1.79 HMDS/nm2 from TGA results.HMDS/HDI/SiO2 hybrid particles exhibited strong hydrophobicity(143°) after modification.Both hybrid particles exhibited good miscibility and dispersibility in apolar solvents relative to unmodified silica nanoparticles." @default.
- W2393392248 created "2016-06-24" @default.
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- W2393392248 date "2012-01-01" @default.
- W2393392248 modified "2023-09-24" @default.
- W2393392248 title "Preparation and characterization of HDI/SiO_2 and HMDS/HDI/SiO_2 hybrid particles" @default.
- W2393392248 hasPublicationYear "2012" @default.
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