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- W2393466196 abstract "Objective: To establish a determination method for imperatorin and asarinin in Eliminating Pain and Stasis Liniment,so as to lay a foundation for its quality standards. Methods: The column was Kromasil C18( 4. 6 mm × 250 mm,5 μm). The mobile phase for determination of imperatorin was methanol-water( 65 ∶ 35),the flow rate was 1. 0 mL /min,and the detective wavelength was 300 nm. The mobile phase for determination of asarinin was acetonitrile-water,gradient elution,the flow rate was 1. 0 mL / min,and the detective wavelength was 287 nm. Results: The linear range of imperatorin and asarinin were 25. 0 ~ 375 ng and 74. 0 ~ 1110 ng respectively. The average recoveries were 98. 96%( n =6) and 96. 12%( n = 6),with RSD = 2. 28% and RSD = 2. 20%. Conclusion: The method is simple operation,highly specific with good reproducibility. This method can provide scientific basis for the quality standards formulating of Eliminating Pain and Stasis Liniment." @default.
- W2393466196 created "2016-06-24" @default.
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- W2393466196 date "2014-01-01" @default.
- W2393466196 modified "2023-09-25" @default.
- W2393466196 title "Determination of Imperatorin and Asarinin in Eliminating Pain and Stasis Liniment by RP-HPLC" @default.
- W2393466196 hasPublicationYear "2014" @default.
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