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- W2393476174 abstract "The sample of human plasma was treated with 0. 01mol · L -1 hydrochloric acid and alcohol first, and then the clenbuterol in the sample was extracted with chloroform from an sodium hydroxid solution of pH 10 11. The combined extracts of CHC13 solution was treated further as described in the procedure, and a 1μ1 portion from the final sample solution of 100μl in alcohol was taken for the determination by GC/MS with the selective ion measurement method. Under the optimum conditions, linearity was held in the range of 0. 1-100ng of clenbuterol in 1μl of the sample solution, and the detection limit (S/N=3) was found to be 0. 05ng. Recovery test was made by the standard addition method and an average value of 95.6% was obtained, and the RSD s (n=6) obtained were less than 6. 82%. The special features of the proposed method were that no pre-derivatization is necessary, and no interference by the base-material was observed. It was proved that this method is simple and accurate, and is feasible to be used as a rapid routine method for the determination of clenbuterol in human plasma and other biological samples." @default.
- W2393476174 created "2016-06-24" @default.
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- W2393476174 date "2004-01-01" @default.
- W2393476174 modified "2023-09-27" @default.
- W2393476174 title "RAPID GC/MS DETERMINATION OF CLENBUTEROL IN HUMAN PLASMA" @default.
- W2393476174 hasPublicationYear "2004" @default.
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