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- W2393722897 abstract "The thermal stability properties and the thermal decomposition reaction kinetics of hydroxylamine sulfate(HAS) were studied at different heating rates(4 ℃/min,7 ℃/min,and 10 ℃/min) by differential scanning calorimetry(DSC) in the range of RT(room temperature)-400℃.The DSC data of the STA simultaneous thermal analyzer were analyzed by Advanced Kinetics and Technology Solutions(AKTS).Then the kinetics parameters including the activation energy,preexponential factor and reaction enthalpy were calculated by the thermal kinetics analysis method.The results showed that self-exothermic decomposition reaction occurred in the air atmosphere.The heat of reaction was 118.8±2.1 kJ/mol. The activation energy was calculated according to the Ozawa method,and its value was 82.45 kJ/mol.Then the relations between differential conversional and activation energy(or preexponential factor) were gained according to the Friedman method,and the reaction enthalpy was calculated as 116.2±1.1 kJ/mol.Finally, the safety process of the hydroxylamine sulfate production was discussed.In the storage and transportation process,the temperature rising should be prevented,or else,the explosion accident of the hydroxylamine sulfate will be initiated by self-exothermic decomposition reaction.The experiment results could be used as reference and guide for the actual industry processes." @default.
- W2393722897 created "2016-06-24" @default.
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- W2393722897 date "2011-01-01" @default.
- W2393722897 modified "2023-09-28" @default.
- W2393722897 title "Study on thermal decomposition kinetics of hydroxylamine sulfate" @default.
- W2393722897 hasPublicationYear "2011" @default.
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