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- W2393740474 abstract "[Aims] 2,3-Dichloro-5-methylpyridine is an important class of chemical intermediates, this study aims to develop a new method for synthesizing 2,3-dichloro-5-methylpyridine and the synthetic process was further optimized.[Methods] 2,3-Dichloro-5-methylpyridine was synthesized from 5-methyl-3,4-diludine-2(1H)-one and chlorine in the presence of FeCl3 and N,N,N',N',N''-pentamethyldiethylenetriamine. The main factors such as catalyst, ligand and temperature were studied. [Results] Under the optimal condition, the yield of 2,3-dichloro-5-methylpyridine was 75%with purity of 99.5%. [Conclusions] This process is simple and safe with little industrial waste, which is suitable for industrial production." @default.
- W2393740474 created "2016-06-24" @default.
- W2393740474 creator A5035059121 @default.
- W2393740474 date "2014-01-01" @default.
- W2393740474 modified "2023-09-25" @default.
- W2393740474 title "Synthesis of 2,3-Dichloro-5-methylpyridine Catalyzed by FeCl_3" @default.
- W2393740474 hasPublicationYear "2014" @default.
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