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- W2393954890 abstract "A synthetic method for tetraalkylmonothiopyrophosphates has been worked out as follows: Tetraalkylmonothiopyrophosphates(2, R=C_2H_5, i-C_4H_9) were synthesized from the reaction of two moles of the corresponding dialkyl phosphonates with one mole of sulfur in carbon tetrachloride in the presence of excess triethylamine. The yields ranged from 65 to 80％. The method can be modified for the synthesis of unsymmetrical diethyl dialkyl monothiopyrophoshpates (6, R=alkyl=i-C_3H_7, i-C_4H_9, sec-C_4H_9). The reaction mechanism was briefly discussed." @default.
- W2393954890 created "2016-06-24" @default.
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- W2393954890 date "1981-01-01" @default.
- W2393954890 modified "2023-09-27" @default.
- W2393954890 title "A SIMPLE SYNTHETIC METHOD OF TETRAALKYL MONOTHIOPYROPHOSPHATES" @default.
- W2393954890 hasPublicationYear "1981" @default.
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