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- W2394051453 abstract "An analytical method was developed for determination of benzo(a)pyrene in oil-tea camellia seed oil by saponification with 2 mol/L KOH-CH3CH2OH solution and extraction with petroleum ether,and then purification by a neutral aluminium column,then determination with HPLC.The determination conditions were as follows: analysis cloumn PAH C18,mobile phase acetonitrile/water(containing 0.5%phosphoric acid)95∶5,flow rate 1.0 mL/min,excitation wavelength 384 nm,emission wavelength 406 nm,column temperature 30 ℃.At fortification levels of 2.00～20.0 μg/kg,recoveries for benzo(a)pyrene varied from 93.0% to 110.0%,the relative standard deviation varied from 2.59% to 9.57%,the limit of detection was 0.2 μg/kg.The method was characterized by simplicity,sensitivity and accuracy." @default.
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- W2394051453 date "2012-01-01" @default.
- W2394051453 modified "2023-09-24" @default.
- W2394051453 title "Saponification-extraction and HPLC determination of benzo(a) pyrenein oil-tea camellia seed oil" @default.
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