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- W2394103619 abstract "Objective: To establish a method for determining the content of Pb,Cd,As,Hg,Cu and Cr in Cervi Cornus Colla.Method: Microwave digestion and inductively coupled plasma-atomic wmission spectrometry(ICP-AES) were adopted to determine the content of Pb,Cd,As,Hg,Cu and Cr in 11 batches of Cervi Cornus Colla.Microwave digestion conditions were as followings: 0-3 min,1 600 W,110 ℃;3-6 min,1 600 W,150 ℃;6-16 min,1 600 W,185 ℃.Determination conditions of ICP-AES were: incident power of 1.4 kW,argon as cooling gas with flow rate of 12 L.min-1,flow rate of carrier gas and auxiliary with 1,0.8 L.min-1,volume of sample enhance 1 mL.min-1.Result: Detection limit of Pb,Cd,As,Hg,Cu and Cr were 0.15,0.01,0.27,0.08,0.03,0.03 mg.kg-1,respectively.recoveries was between 90%-112%,precision and repeatability were in line with detection requirments.Cd,As and Hg were not detected in each sample,apart from sample from F was not detected Pb,Pb,Cu and Cr were detected in other samples,the content of Cr was high in some samples.Conclusion: This method was accurate,fast and suitable for determination of harmful elements in glue herbs." @default.
- W2394103619 created "2016-06-24" @default.
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- W2394103619 date "2013-01-01" @default.
- W2394103619 modified "2023-09-24" @default.
- W2394103619 title "Determination of Harmful Elements in Cervi Cornus Colla Based on Microwave Digestion and ICP-AES Technology" @default.
- W2394103619 hasPublicationYear "2013" @default.
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