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- W2394294927 abstract "Objective To analyze the contents of 17 amino acids in MACA using pre-column derivatization method. Methods The amino acids in MACA were pretreated with 2,4-dinitro-fluorobenzene and their derivatives were analyzed on Waters 600 HPLC using Symmetry C18 column. Gradienteluents consisted of sodium acetate solution(pH=6.4) with 1% N,N-dimethylformamide, acetonitrile and water(1 ∶ 1). The Detection wavelength was 360nm and column temperature was 35℃. Results The calibration curves for 18 amino acidshad good linearity(r=0.9995 ~ 1,n=5). The mean recoveries of 18 amino acids were 99.54%-101.84% with RSD 0.38%-1.82%(n=6). Conclusion The method is quick, simple for the content analysis of the amino acids in the injections." @default.
- W2394294927 created "2016-06-24" @default.
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- W2394294927 date "2014-01-01" @default.
- W2394294927 modified "2023-09-26" @default.
- W2394294927 title "Contents of 18 amino acids in MACA using pre-column derivatization method" @default.
- W2394294927 hasPublicationYear "2014" @default.
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