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- W2394414317 abstract "Ahigh-performance liquid chromatographic method was developed for determination of metronidazole in eggsand milk.The sample was extracted with ethyl acetate.The extract evaporated and redissolved in a mixture of hexane and ethyl acetate(2∶1).The extract was cleaned up by solid phase extraction on a silica cartridge.The eluted was evaporated to dryness with nitrogen followed by dissolution with HPLC eluent and detection with UV. The limit of detection for metronidazole in eggsand milk was 1 μg/kg.The mean recoveries of metronidazole was 65.8% and 75.4% respectively in eggsand milk at the level of 1 μg/kg with the intra-day relative deviation less than 15%.The method was applied to layersgiven feed containted 0.025% metronidazole for 7 days.Residues of metronidazole and its metabolite were detected in egg shortly after the administration period but not 14 days later.The results showed that this method was accurate and feasible enough to determinate the residue of metronidazole with simple samples pre-treatment." @default.
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- W2394414317 date "2006-01-01" @default.
- W2394414317 modified "2023-09-26" @default.
- W2394414317 title "Developmentof a High-performance Liquid Chromatographic Method for Detection of Metronidazole Residues in Eggs and Milk" @default.
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