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- W2394996627 abstract "Abstract A liquid chromatographic method for the assay of oxytetracycline in premixes and veterinary products is described. Premix samples are extracted with acidified methanol, diluted with mobile phase, and filtered before chromatography on a C-8, reverse phase .column. The assay method separates oxytetracycline from epioxytetracycline, tetracycline, and chlortetracycline. Total elution time for oxytetracycline is less than 5 min at 1.5 mL/min. Five spiked premix samples each of 2 and 50 g/lb had a coefficient of variation of 3.5 and 4.5% and a mean recovery of 99 and 104%, respectively. The results of premixes and veterinary products assayed by this method compared closely with those of the same samples assayed by the official AOAC microbiological method." @default.
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- W2394996627 date "1986-01-01" @default.
- W2394996627 modified "2023-10-14" @default.
- W2394996627 title "Determination of Oxytetracycline in Premixes and Veterinary Products by Liquid Chromatography" @default.
- W2394996627 doi "https://doi.org/10.1093/jaoac/69.1.28" @default.
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