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• W2395292626 startingPage "1613" @default.
• W2395292626 abstract "Initiators for continuous activator regeneration atom transfer radical polymerization (ICAR ATRP) of acrylonitrile was first conducted at various ambient temperatures (30–45 °C). The key to success is ascribed to the usage of an appropriate low temperature radical initiator (2,2′-azobis(2,4-dimethylvaleronitrile)) and a high reactivity catalytic system (CuBr2/Me6TREN). The molar ratio of Cu catalyst to AN as low as 1:20000 was used to prepare well-defined polyacrylonitrile with controlled molecular weight and a narrow polydispersity index range of 1.08–1.30, while the monomer conversion was up to ca. 98%. The apparent activation energy of the polymerization was calculated to be 128.45 kJ/mol, suggesting that the polymerization strongly depended on reaction temperature. The very high chain-end functionality of the resultant polymer was confirmed by 1H-NMR and GPC analyses as well as chain extension reaction." @default.
• W2395292626 created "2016-06-24" @default.
• W2395292626 creator A5016515083 @default.
• W2395292626 creator A5035358476 @default.
• W2395292626 date "2013-11-08" @default.
• W2395292626 modified "2023-10-16" @default.
• W2395292626 title "ICAR ATRP of acrylonitrile utilizing a moderate temperature radical initiator" @default.
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• W2395292626 doi "https://doi.org/10.1007/s10118-013-1348-y" @default.
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