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• W2395758925 abstract "We synthesized LiNi0.5Mn1.5O4 with the Fd-3m space group by using oxalate co-precipitation. The structure and morphology, electrochemical properties of the obtained LiNi0.5Mn1.5O4 was investigated by XRD, SEM, galvanostatic charge/discharge testing and electrochemical impedance spectroscopy, respectively. Li/Ni antisite defects appeared in the disordered LiNi0.5Mn1.5O4. Using Rietveld refinement, we found that the second phase generated was Ni6MnO8 rather than LixNi1−xO. During the phase transformation, if sufficient Ni6MnO8 was produced, the spinel structure could not sustain more Li in the original crystal lattice, which generated an unstable structure in which excess Li existed in Li2MnO3. Due to the high capacity of Li2MnO3, the capacity of spinel LiNi0.5Mn1.5O4 with Li2MnO3 is expected to further improve." @default.
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• W2395758925 date "2016-10-01" @default.
• W2395758925 modified "2023-10-09" @default.
• W2395758925 title "Phase transformation during synthesis of LiNi0.5Mn1.5O4 by oxalate co-precipitation" @default.
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• W2395758925 doi "https://doi.org/10.1016/j.matlet.2016.05.116" @default.
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