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- W2399691098 abstract "Much interest has been paid to cyclic diaryliodonium salts as bis(electrophile)s in transition-metal-catalyzed annulation reactions to produce polycyclic (hetero)aromatic hydrocarbons. Herein, we report that dibenziodolium triflates smoothly react with potassium thioacetate in the presence of CuCl2 in THF or DMSO at 100–110 °C to afford the corresponding dibenzothiophenes in good-to-high yields. The coupling reaction tolerates reactive functional groups such as chloro and cyano and serves as a facile and reliable method for the synthesis of unsymmetrical dibenzothiophenes." @default.
- W2399691098 created "2016-06-24" @default.
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- W2399691098 date "2016-05-23" @default.
- W2399691098 modified "2023-10-07" @default.
- W2399691098 title "Copper-Catalyzed Double S-Arylation of Potassium Thioacetate with Dibenziodolium Triflates: Facile Synthesis of Unsymmetrical Dibenzothiophenes" @default.
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- W2399691098 doi "https://doi.org/10.1002/ejoc.201600357" @default.
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