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- W2399693383 abstract "High pressure strongly favors the highest-density polymorph Z of active pharmaceutical ingredient 2-(2,6-xylidino)-5,6-dihydro-4H-1,3-thiazine hydrochloride (xylazine hydrochloride, XylHCl) up to about 0.1 GPa only, but still higher pressure destabilizes this structure. Above 0.1 GPa, XylHCl preferentially crystallizes as solvates with CH2Cl2, CHCl3, or (CH3)2CHOH depending on the solvent used. However, when XylHCl·H2O is dissolved in any of these solvents, the high-pressure crystallizations yield the hydrate XylHCl·H2O only. The single crystals of the CH2Cl2, CHCl3, and (CH3)2CHOH solvates could be grown in situ in a diamond anvil cell, which allowed their structure determination from the single-crystal diffraction data. At 0.4 GPa the XylHCl·H2O hydrate undergoes a pressure-induced phase transition doubling the unit cell dimensions." @default.
- W2399693383 created "2016-06-24" @default.
- W2399693383 creator A5038667320 @default.
- W2399693383 creator A5048564373 @default.
- W2399693383 creator A5049486183 @default.
- W2399693383 date "2016-06-14" @default.
- W2399693383 modified "2023-10-17" @default.
- W2399693383 title "Pressure-Stabilized Solvates of Xylazine Hydrochloride" @default.
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- W2399693383 doi "https://doi.org/10.1021/acs.cgd.6b00264" @default.
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