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- W2403375006 abstract "Abstract A liquid chromatographic method is described for the analysis of RH-5992 (N'-t-butyl-N'-[3,5-dimethylbenzoyl]- N-[4-ethylbenzoyl] hydrazine) from various terrestrial and aquatic forestry matrixes and stream water. The processed soils, Hitter, oak foliage, sediment, aquatic plants, and fish were extracted with a mixture of acetone and water; balsam fir needles were extracted with acidified methanol solution; stream water was extracted with dichloromethane. Aliquots of crude extracts were solvent partitioned, concentrated, and cleaned up by using Florisil or Prepsep-NH2 columns. After fractional elution of the columns with hexane-ethyl acetate as the eluent, the eluates were analyzed on a liquid chromatograph equipped with a diode-array UV detector set at 236 nm, using an RP-8,10 μm column with a mobile phase of acetonitrile- dioxane-water. Fir needles required methanol in addition to the 3 solvents in the mobile" @default.
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- W2403375006 date "1993-05-01" @default.
- W2403375006 modified "2023-09-25" @default.
- W2403375006 title "Liquid Chromatographic Determination of RH-5992, an Ecdysone Agonist, in Some Forestry Matrixes" @default.
- W2403375006 doi "https://doi.org/10.1093/jaoac/76.3.668" @default.
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