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- W2403972793 abstract "The crystal structure of APA 2(Zn 3(HPO 4)4(H 2O) 2) (APA = 2-amino-1-phenylene- ammonium, C 6H9N2 + ) (1), as prepared by a predominantly non-aqueous synthesis, is described and compared to related compounds. 1 is built up from an alternating array of ZnO 4 and HPO 4 tetrahedra sharing vertices as Zn-O-P bonds to generate infinite anionic sheets. Within these sheets, polyhedral 4-, 6- and 8-rings are apparent. The negative charge of the inorganic layer is balanced by singly-protonated APA template cations and water molecules are also present. The components are linked by N t-HLOf, O f-HLOw, Ow-HLOf and O f-HLNt (t = template, f = framework, w = water) hydrogen bonds: the last of these represents an unusual framework-to-template interaction. Weak C t-HLOf links may also play a role in consolidating the structure. Crystal data: 1 (C 12 H26 N4O18 P4Zn 3), Mr = 834.36, monoclinic, C2/ c (No. 15), Z = 4, a = 20.194 (8) A, b = 8.682 (3) A, c = 15.123 (6) A, β = 91.510 (11)°, V = 2650.5 (17) A 3 , R(F) = 0.048, wR (F 2 ) = 0.112." @default.
- W2403972793 created "2016-06-24" @default.
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- W2403972793 date "2012-01-01" @default.
- W2403972793 modified "2023-09-26" @default.
- W2403972793 title "LO and Synergic Framework-to-Template O-HLN Hydrogen Bonds and C-HLO Interactions (APA = 2-Amino-1-phenyleneammonium, C 6H9N2 + )" @default.
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