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- W2407367069 abstract "The parameters affecting the separation and quantification of trimethylsilyl ethers of mono- and diglycerides have been investigated by gas-liquid chromatography with QF-1 and SE-30 as stationary phases and a flame ionization detector. Results have been compared with those obtained earlier for triglycerides. The isothermal characteristics of a range of trimethylsilyl ethers of mono- and diglycerides on both stationary phases showed that log retention volume was directly proportional to number and inversely proportional to absolute temperature. However, glyceride derivatives with lower numbers deviated from these relationships. By using various rates of programmed temperature rise, we have determined the elution temperatures (Kelvin scale) of the mono- and diglyceride trimethylsilyl ethers relative to that of glycerol trilaurate. The carbon equivalent of a trimethylsilyl group is defined and shown to be useful in comparing the chromatographic properties of different glyceride classes. Weight and molar correction factors have been obtained and used to analyze diglycerides derived from egg and bovine brain lecithins." @default.
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- W2407367069 date "1969-01-01" @default.
- W2407367069 modified "2023-09-23" @default.
- W2407367069 title "Separation of mono- and diglycerides by gas-liquid chromatography" @default.
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- W2407367069 doi "https://doi.org/10.1016/s0022-2275(20)42646-x" @default.
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