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- W2410789593 abstract "A rapid and direct liquid chromatographic (LC) technique is described for the determination of a eutectic mixture of diphenyl oxide and biphenyl such as Dowtherm A thermal heating fluid (THF) in oleochemicals and palm olein. Analysis is performed with an RP-18 column with fluorescence detection (excitation at 247 nm and emission at 310 nm). The isocratic mobile phase (1.0 mL/min) consists of methanol and water (90 + 10, v/v). A linear calibration model (correlation coefficient = 0.9999) was developed directly from used Dowtherm A THF with the biphenyl peak (4.70 min) as a marker. Average recoveries from spiked glycerin, fatty alcohol mixture, methyl ester mixture, fatty acids, and palm olein were 90.9-108.7%, with a detection limit of 0.1 microgram/mL. The technique requires no prior sample cleanup nor extraction steps and is good for quality assurance purposes." @default.
- W2410789593 created "2016-06-24" @default.
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- W2410789593 date "1999-07-01" @default.
- W2410789593 modified "2023-09-27" @default.
- W2410789593 title "Liquid Chromatographic Detection of Dowtherm A Contamination in Oleochemicals and Edible Oils" @default.
- W2410789593 doi "https://doi.org/10.1093/jaoac/82.4.893" @default.
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