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• W2415667799 abstract "In this work, the poly(methyl methacrylate-co-pentafluorophenyl acrylate) [P(MMA-co-PnFPA)] copolymer by dispersion polymerization in supercritical carbon dioxide was prepared. The physicochemical properties for the P(MMA-co-PnFPA) were investigated with varied mole ratios of MMA vs PnFPA (20:1, 25:1 and 30:1), and 1.0 wt%, 2.0 wt% and 4.0 wt% AIBN amounts. Experimental cloud-point data up to 453 K and 220 MPa are measured for binary and ternary mixtures of P(MMA-co-PnFPA) in supercritical CH2F2, CHF3 and CHClF2. Phase behavior of binary systems for the P(MMA-co-PnFPA) [mole ratio = 25:1, AIBN: 1.0 wt% (Mw = 173,000), 2.0 wt% (Mw = 93,600), and 4.0 wt% (Mw = 74,600)] + CH2F2 (or CHF3 and CHClF2) mixtures at temperature range from 333 K to 434 K and pressure up to 153 MPa are measured the upper critical solution temperature (UCST) type behavior with negative slope for the P(MMA-co-PnFPA) + CH2F2, and lower critical solution temperature (LCST) type curve with positive slope for the P(MMA-co-PnFPA) + CHF3 and P(MMA-co-PnFPA) + CHClF2 mixtures. Cloud-point curves for the P(MMA-co-PnFPA) [mole ratio = 20:1 (Mw = 170,000), 25:1 (Mw = 173,000), and 30:1 (Mw = 228,000); 1.0 wt% AIBN] + supercritical (CH2F2, CHF3 and CHClF2) mixtures show a negative slope for the P(MMA-co-PnFPA) + CH2F2, and a positive slope for the P(MMA-co-PnFPA) + CHF3 and P(MMA-co-PnFPA) + CHClF2 mixtures at temperature to 453 K and pressure up to 160 MPa. Also, the impact of MMA (or CHClF2) on phase behavior for the P(MMA-co-PnFPA) (25:1; 1.0 wt% AIBN) + CH2F2 mixtures are measured in changes of the pressure-temperature (p, T) slope from UCST behavior to LCST behavior, and with MMA (or CHClF2) cosolvent concentrations of (0.0–28.9) wt% (or CHClF2: 0.0–97.2 wt%)." @default.
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• W2415667799 date "2017-02-01" @default.
• W2415667799 modified "2023-09-26" @default.
• W2415667799 title "Cloud-point measurement of binary and ternary mixtures for the P(MMA-co-PnFPA) in supercritical fluoric solvents" @default.
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• W2415667799 doi "https://doi.org/10.1016/j.supflu.2016.05.029" @default.
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