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• W2415674813 abstract "3-Halodiazirine-3-carboxylic acids (c-CN2XCOOH, X = Cl or Br) were prepared from their esters and converted to the corresponding sodium salts. Collision-induced dissociation (CID) of the carboxylate ions led exclusively to the loss of CO2 and the resulting c-CN2X– ions dissociated to c-CN2 carbene at low energies. The bond dissociation energy (BDE) for c-CN2Br– was found to be less than 8 kcal/mol using CID of the anion generated by electrospray ionization of the carboxylate. The analogous difluoro system (CF2XCOOH/CF2X–/CF2) exhibits similar dissociative behavior. All experimental BDEs are in very good agreement with MP4/aug-cc-pVTZ calculations." @default.
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• W2415674813 date "2014-10-08" @default.
• W2415674813 modified "2023-10-01" @default.
• W2415674813 title "Evidence for the Cyclic CN2 Carbene in the Gas Phase" @default.
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• W2415674813 doi "https://doi.org/10.1021/ol5027602" @default.
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