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• W2415911593 endingPage "2100" @default.
• W2415911593 startingPage "2091" @default.
• W2415911593 abstract "Macrocyclic oligoester structures based on a cyclotetrasiloxane core consisting of tricyclic (60+ atoms) and pentacycylic (130+ atoms) species were identified as the major components of a lipase-mediated transesterification reaction. Moderately hydrophobic solvents with log P values in the range of 2-3 were more suitable than those at lower or higher log P values. Temperature had little effect on total conversion and yield of the oligoester macrocycles, except when a reaction temperature of 100 °C was employed. At this temperature, the amount of the smaller macrocycle was greatly increased, but at the expense of the larger oligoester. For immobilized lipase B from Candida antarctica (N435), longer chain length esters and diols were more conducive to the synthesis of the macrocycles. Langmuir isotherms indicated that monolayers subjected to multiple compression/expansion cycles exhibited a reversible collapse mechanism different from that expected for linear polysiloxanes." @default.
• W2415911593 created "2016-06-24" @default.
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• W2415911593 date "2015-06-25" @default.
• W2415911593 modified "2023-09-23" @default.
• W2415911593 title "Macrocyclic Oligoesters Incorporating a Cyclotetrasiloxane Ring" @default.
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• W2415911593 doi "https://doi.org/10.1021/acs.biomac.5b00518" @default.
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