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- W2416697913 abstract "Superhydrophobic coatings were prepared using 3-(heptafluoroisopropoxy)- propyltrimethoxysilane (HFIP-TMS) treated diatomaceous earth (DE) particles with high molecular mass polystyrene or poly(vinyl acetate) as polymer binders. DE is a highly hydrophilic material and treatment of the DE with HFIP-TMS turned it into superhydrophobic diatomaceous earth (HFIP-DE). Thermogravimetric analysis (TGA) was used to determine the amount of grafted fluorosilane on the surface of the DE particles. The results showed that approximately 1.8% of HFIP-TMS grafted onto the surface of DE particles resulted in superhydrophobicity with contact angles as high as 164° for the particles themselves and also in coatings. Fourier transformed infrared spectroscopy (FTIR) was used to confirm the presence of HFIP-TMS on the surface of DE particles. The development of the hydrophobicity in the coatings with either polystyrene (PS) or poly(vinyl acetate) (PVAc) as binders was followed as a function of the particle loading using contact angle measurements and scanning electron microscopy. It was found that for these model DE-binder systems, the contact angles of the coatings were independent of the polymers used as long as the particle loading was greater than a minimum amount (∼40% treated DE particles). It was also found that more treated DE particles moved to the air interface as the particle loadings in the coatings increased and then levelled off." @default.
- W2416697913 created "2016-06-24" @default.
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- W2416697913 date "2016-11-01" @default.
- W2416697913 modified "2023-09-25" @default.
- W2416697913 title "Development of superhydrophobicity in fluorosilane-treated diatomaceous earth polymer coatings" @default.
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- W2416697913 doi "https://doi.org/10.1016/j.apsusc.2016.06.009" @default.
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