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- W2417364047 abstract "A method to determine the water vapor pressure over a corrosive substance was developed and tested with 85.5 ± 0.4% phosphoric acid. The water vapor pressure was obtained at a range of temperatures from ∼25 ℃ to ∼200 ℃ using Raman spectrometry. The acid was placed in an ampoule and sealed with a reference gas (either hydrogen or methane) at a known pressure (typically ∼0.5 bar). By comparing the Raman signals from the water vapor and the references, the water pressure was determined as a function of temperature. A considerable amount of data on the vapor pressure of phosphoric acid are available in the literature, to which our results could successfully be compared. A record value of the vapor pressure, 3.40 bar, was determined at 210 ℃. The method required a determination of the precise Raman scattering ratios between the substance, water, and the used reference gas, hydrogen or methane. In our case the scattering ratios between water and reference ν 1 Q-branches were found to be 1.20 ± 0.03 and 0.40 ± 0.02 for H 2 and CH 4 , respectively." @default.
- W2417364047 created "2016-06-24" @default.
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- W2417364047 date "2016-06-07" @default.
- W2417364047 modified "2023-10-18" @default.
- W2417364047 title "Determination of Water Vapor Pressure Over Corrosive Chemicals Versus Temperature Using Raman Spectroscopy as Exemplified with 85.5% Phosphoric Acid" @default.
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- W2417364047 doi "https://doi.org/10.1177/0003702816652362" @default.
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