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- W2433444100 abstract "The title compound, [Re 6 Se 8 {O 3 SC 6 H 4 (CH 3 )}{P(C 2 H 5 ) 3 } 5 ](CH 3 C 6 H 4 SO 3 )·2CH 2 Cl 2 , contains the face-capped hexanuclear [Re 6 (μ 3 -Se) 8 ] 2+ cluster core. The [Re 6 Se 8 ] 2+ cluster core displays a non-crystallographic center of symmetry and is bonded through the Re III atoms to five triethylphosphane ligands and one p -toluenesulfonate ligand. One p -toluenesulfonate counter-ion and two dichloromethane solvent molecules are also present in the asymmetric unit. One of the ethyl chains of one triethylphosphane ligand and one of the CH 2 Cl 2 solvent molecules are disordered over two sets of sites (occupancy ratios 0.65:0.35 and 0.5:0.5, respectively). The Re—O(sulfonate) bond length of 2.123 (5) Å is similar to other Re—O bond lengths of hexanuclear rhenium chalcogenide clusters containing other O -donor ligands such as dimethyl sulfoxide (DMSO), dimethylformamide (DMF) and hydroxide." @default.
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- W2433444100 date "2015-08-06" @default.
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- W2433444100 title "Crystal structure of octa-μ<sub>3</sub>-selenido-(<i>p</i>-toluenesulfonato-κ<i>O</i>)pentakis(triethylphosphane-κ<i>P</i>)-<i>octahedro</i>-hexarhenium(III)<i>p</i>-toluenesulfonate dichloromethane disolvate" @default.
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- W2433444100 doi "https://doi.org/10.1107/s2056989015014334" @default.
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