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- W245770922 abstract "The reactions of pentafluorophenyl, 2,2,3,3-tetrafluoropropyl alcohol, and 2,2,3,3,4,4,5,5-octafluoropentyl alcohol with carbon tetrachloride in the presence of aluminum chloride were investigated. The main products from the reaction of pentafluorophenol with these reagents are pentafluorophenoxy-trichloromethane, di(pentafluorophenol) carbonate, and tri(pentafluorophenoxy)-chloromethane. The ratios of the products depend on the reaction conditions. The use of a large excess of carbon tetrachloride leads to the preferential formation of pentafluorophenoxytrichloromethane. The addition of water promotes the formation of di(pentafluorophenyl) carbonate. When heated with carbon tetrachloride and aluminum chloride and subsequently treated with water, 2,2,3,3-tetrafluoropropyl and 2,2,3,3,4,4,5,5-octafluoropentyl alcohols are converted into di(2,2,3,3-tetrafluoropropyl)carbonate and di(2,2,3,3,4,4,5,5-octofluoropentyl) carbonate respectively." @default.
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- W245770922 date "1988-12-20" @default.
- W245770922 modified "2023-09-28" @default.
- W245770922 title "Reactions of pentafluorophenyl and polyfluorinated alcohols with carbon tetrachloride in the presence of aluminum chloride" @default.
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