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- W245876936 abstract "Addition of vanadium to the divacant {gamma}-(HSiW{sub 10}O{sub 36}){sup 7{minus}} anion gives quantitatively the {gamma}-decatungsto-1,2-divanadosilicate (SiV{sub 2}W{sub 10}O{sub 40}){sup 6{minus}} parent complex. This complex is stable in nonaqueous solution but isomerizes in water. The isomerization was followed by polarography, and depending on the experimental conditions, three geometrical isomers of (SiV{sub 2}W{sub 10}O{sub 40}){sup 6{minus}} were prepared (as pure compounds for two of them). These isomers are characterized by their IR spectra and their {sup 183}W, {sup 51}V, and {sup 29}Si NMR spectra. All have the {beta}-structure with the two vanadium atoms in positions (8,12), (3,12), and (3,8), respectively." @default.
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- W245876936 date "1991-03-01" @default.
- W245876936 modified "2023-09-26" @default.
- W245876936 title "Disubstituted tungstosilicates. 2. .gamma.- and .beta.-isomers of tungstovanadosilicate, [SiV2W10O40]6-: syntheses and structure determinations by tungsten-183, vanadium-51 and silicon-29 NMR spectroscopy" @default.
- W245876936 doi "https://doi.org/10.1021/ic00005a020" @default.
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