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• W2460185093 abstract "We report the design of a radio-frequency induction-heated rod casting furnace that permits the preparation of polycrystalline ingots of intermetallic compounds under ultra-high vacuum compatible conditions. The central part of the system is a bespoke water-cooled Hukin crucible supporting a casting mold. Depending on the choice of the mold, typical rods have a diameter between 6 mm and 10 mm and a length up to 90 mm, suitable for single-crystal growth by means of float-zoning. The setup is all-metal sealed and may be baked out. We find that the resulting ultra-high vacuum represents an important precondition for processing compounds with high vapor pressures under a high-purity argon atmosphere up to 3 bars. Using the rod casting furnace, we succeeded to prepare large high-quality single crystals of two half-Heusler compounds, namely, the itinerant antiferromagnet CuMnSb and the half-metallic ferromagnet NiMnSb." @default.
• W2460185093 created "2016-07-22" @default.
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• W2460185093 date "2016-06-01" @default.
• W2460185093 modified "2023-10-18" @default.
• W2460185093 title "Ultra-high vacuum compatible induction-heated rod casting furnace" @default.
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• W2460185093 doi "https://doi.org/10.1063/1.4954926" @default.
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• W2460185093 hasPublicationYear "2016" @default.
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