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- W2464486585 abstract "As part of our ongoing research for molecular structures binding to the translocator protein (TSPO 18 kDa), we investigated the preparation of a number of new 2,4,5‐trisubstituted pyridines as novel building blocks. In particular, 5‐amino‐2‐halo‐4‐phenoxypyridines ( 11 , 12 , 13 ) were designed as key intermediates for the synthesis of the recently developed TSPO ligand 6‐F‐PBR28 and its fluorine‐18‐labeled version for positron emission tomography, 6‐[ 18 F]F‐PBR28. We hereby report the chemical preparation as well as the 1 H and 13 C NMR spectroscopic data of polysubstituted pyridines 2 , 3 , 4 , 5 , 6 , 7 , 7b , 8 , 9 , 10 , 11 , 12 , 13 , 14 . The latter demonstrates dramatic changes in electron density repartition of the aromatic ring upon substitution." @default.
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- W2464486585 date "2013-11-18" @default.
- W2464486585 modified "2023-10-15" @default.
- W2464486585 title "Novel 2,4,5‐Trisubstituted Pyridines as Key Intermediates for the Preparation of the TSPO Ligand 6‐F‐PBR28: Synthesis and Full <sup>1</sup>H and <sup>13</sup>C NMR Characterization" @default.
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- W2464486585 doi "https://doi.org/10.1002/jhet.1723" @default.
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