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- W2464930147 abstract "Chemical co-precipitation method was used to prepare Gd 2 Zr 2 O 7 powders. The powders were then heated in air at 1500°C, 1510°C, 1525°C, 1530°C, 1550°C, 1575°C, 1600°C for 5 h, and 1575°C, 1600°C for 10 h, respectively. The samples after heat treatment were characterized by X-ray diffraction and Raman spectroscopy. X-ray diffraction patterns reveal that order-disorder transition of Gd 2 Zr 2 O 7 occurs between 1550°C and 1575°C. Prior to the transition, the relative intensity of peaks corresponding to the super-lattice of pyrochlores increases with the increasing temperature. On the other hand, Raman spectra give an inconsistent result from the X-ray diffraction data. No appreciable difference can be observed for all the samples though with peaks broadening as temperature increases. The spectra of the samples indicated as fluorite structure in X-ray diffraction patterns appear with six resolvable peaks which is quite different from the spectrum of ideal fluorite structure." @default.
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- W2464930147 date "2016-07-01" @default.
- W2464930147 modified "2023-09-23" @default.
- W2464930147 title "Influence of Temperature on the Order-Disorder Transition in Gd<sub>2</sub>Zr<sub>2</sub>O<sub>7</sub>" @default.
- W2464930147 doi "https://doi.org/10.4028/www.scientific.net/kem.697.386" @default.
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