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- W2466572571 abstract "The synthesis of aminomethylphosphine-metal complexes have opened a new perspective to the catalytic applications of organic compounds. Magnetic Fe3O4 nano-core was synthesized using the closed quartz tube with Teflon cover and microwaved 200°C for 1h with power controlled instrument set to max. 600W. Novel nano-composite supported; Fe3O4@SiO2(CH2)3NHArN(CH2PPh2)2 and Fe3O4@SiO2(CH2)3N(CH2PPh2)2 type bis(diphenylphosphinomethyl)amino ligands and their Pd(II) complexes have been synthesized and characterized with FT-IR, SEM, EDX, TEM, UV-Visible, XRD and TG/DTA techniques. All the complexes were used as heterogeneous catalysts in the oxidation of 2-methyl naphthalene (2MN) to 2-methyl-1, 4-naphthoquinone (vitamin K3, menadione, 2MNQ) in the presence of hydrogen peroxide and acetic acid. Selectivity reached about 55-60% with a conversion of 90-96% using the nano-magnetite supported aminomethylphosphine-Pd(II) complexes. The complexes were very active in three times in the catalytic recycling experiments in five catalytic cycles." @default.
- W2466572571 created "2016-07-22" @default.
- W2466572571 creator A5075325513 @default.
- W2466572571 date "2016-12-01" @default.
- W2466572571 modified "2023-10-16" @default.
- W2466572571 title "Synthesis of Fe 3 O 4 @SiO 2 @OSi(CH 2 ) 3 NHRN(CH 2 PPh 2 ) 2 PdCl 2 type nanocomposite complexes: Highly efficient and magnetically-recoverable catalysts in vitamin K 3 synthesis" @default.
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- W2466572571 doi "https://doi.org/10.1016/j.foodchem.2016.06.093" @default.
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