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- W2467043311 abstract "The present work reports the effect of reaction time on solvothermal synthesis of copper sulfides from CuCl 2 ·2H 2 O and thiourea with various compositions and morphologies using ethylenediamine as solvent at 120 °C. X-ray diffraction patterns of the products at different durations shows the development of different stoichiometric composition of copper sulfides in where Cu:S ratio increases from 1.39 to 1.79 indicating transformation of Cu 39 S 28 to Cu 7 S 4 . As inferred by EDX and XPS studies of the final products. SEM shows the growth of bundles of nanorods of length ≈1 μ m and diameter in nanometer range are observed after 6 h. On increasing the reaction duration to 9 h, nanorods tends to combines with each other and growth occurs in six directions and after 12 h leads to the formation of flower-like morphology of copper sulfide. The optical properties of these products also have been studied." @default.
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- W2467043311 date "2008-03-01" @default.
- W2467043311 modified "2023-09-25" @default.
- W2467043311 title "Solvothermal Growth of Flower-Like Morphology from Nanorods of Copper Sulfides" @default.
- W2467043311 doi "https://doi.org/10.1166/jnn.2008.18221" @default.
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