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• W2468006215 abstract "We report a new strategy for the direct coupling of Solid-Phase Microextraction (SPME) with mass spectrometry, based on thermal desorption of analytes extracted on the fibers, followed by ionization by a dielectric barrier discharge ionization (DBDI) source. Limits of detection as low as 0.3 pg/mL and a linear dynamic range of ≥3 orders of magnitude were achieved, with a very simple and reproducible approach. Different from direct analysis in real time (DART), desorption electrospray ionization (DESI), or low-temperature plasma (LTP), the desorption of the analytes from the SPME devices in our setup is completely separated from the ionization event. This enhances the reproducibility of the method and minimizes ion suppression phenomena. The analytes were quantitatively transferred from the SPME to the DBDI source, and the use of an active capillary ionization embodiment of the DBDI source greatly enhanced the ion transmission to the MS. This, together with the extraordinary sensitivity of DBDI, allowed subpg/mL sensitivities to be reached and to skip conventional and time-consuming chromatographic separation." @default.
• W2468006215 created "2016-07-22" @default.
• W2468006215 creator A5001571695 @default.
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• W2468006215 creator A5042577413 @default.
• W2468006215 date "2016-07-01" @default.
• W2468006215 modified "2023-10-18" @default.
• W2468006215 title "Direct Coupling of Solid-Phase Microextraction with Mass Spectrometry: Sub-pg/g Sensitivity Achieved Using a Dielectric Barrier Discharge Ionization Source" @default.
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• W2468006215 doi "https://doi.org/10.1021/acs.analchem.6b01507" @default.
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• W2468006215 hasPublicationYear "2016" @default.
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