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• W2468952893 endingPage "2264" @default.
• W2468952893 startingPage "2257" @default.
• W2468952893 abstract "Abstract Synthesis and characterisation of a disubstituted phenanthroline, “dbt‐phen” (“dbt‐phen”, 2,9‐di(benzothiazolino)‐1,10‐phenanthroline) 1 and its Cu I , Cu II , Ni II , Zn II and Fe II complexes are reported. Three different coordination modes of the ligand viz., bis(didentate), tridentate and tetradentate are observed. Under various experimental conditions, 1 forms a double‐stranded dicopper(I)helicate, [Cu I 2 (dbt‐phen) 2 ] 2+ 2 ; a mono(dbt‐phen) copper(II) complex, [Cu II (dbt‐phen)(H 2 O) 2 ] 2+ 3, a Ni II complex [Ni(dbt‐ phen)(NCMe) 2 (OH 2 )] 2+ 4 , a bis(dbt‐phen) zinc(II) complex, [Zn II ( dbt‐phen ) 2 ] 2+ 5 and a pseudo‐octahedral complex [Fe II (dbt‐phen)Br 2 ] 6 . Crystal packing feature of the dicopper helicate [Cu I ( dbt‐phen )] 2 [BF 4 ] 2 , 2 +[BF 4 ] 2 reveals novel short contacts between BF 4 − ions and the hydrogens of the phenyl rings leading to the peculiar double stranded and helical topology. The complex [Cu II ( dbt‐phen )(OH 2 ) 2 (ClO 4 )][ClO 4 ], 3 +[ClO 4 ] exhibits both intra‐ and inter‐molecular H‐bonding interactions. 1 H NMR spectral features of the ligand, copper(I) and zinc(II) complexes indicate that the free ligand and the copper(I) complex retain their solid state structures whereas the zinc(II) complex undergoes structural changes in solution." @default.
• W2468952893 created "2016-07-22" @default.
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• W2468952893 date "2016-07-01" @default.
• W2468952893 modified "2023-10-16" @default.
• W2468952893 title "Structural and NMR Spectroscopic Investigations of Cu^I , Cu^II , Ni^II , Zn^II and Fe^II Complexes of 2, 9-Di-(Benzothiazolino)-1,10-Phenanthroline" @default.
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• W2468952893 doi "https://doi.org/10.1002/slct.201600505" @default.
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