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• W2469374016 abstract "Chiral high-performance liquid chromatography (HPLC) separation of trans-bis[2-(2-pyridyl)aminophenolato] dichlorocyclotriphosphazene was achieved and the absolute configuration of was assigned to be S,S by single-crystal X-ray structural analysis. The optically pure 1,2-diphenyl-1,2-ethanediolate derivatives (+)- and (-)- were synthesized by the reactions of and with (R,R)-hydrobenzoin, respectively, in refluxing toluene in the presence of an excess amount of triethylamine and a catalytic amount of 4-(dimethylamino)pyridine. The racemization of the enantiomers of and the epimerization of diastereomers of 2 were not observed in refluxing toluene neither under acidic nor basic conditions. The stereochemistry of was confirmed by the crystal structure of (+)- and bis[(4-methyl-2-pyridyl)oxy]cyclotriphosphazene derived from . Chirality 28:556-561, 2016. © 2016 Wiley Periodicals, Inc." @default.
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• W2469374016 date "2016-06-07" @default.
• W2469374016 modified "2023-09-27" @default.
• W2469374016 title "Chiral HPLC Separation, Absolute Structural Elucidation, and Determination of Stereochemical Stability of<i>trans</i>-Bis[2-(2-pyridinyl)aminophenolato] Cyclotriphosphazene" @default.
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• W2469374016 doi "https://doi.org/10.1002/chir.22612" @default.
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