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- W2469852445 abstract "The intercalation of H2SO4 into graphite during chemical oxidiation by gaseous oxidizers (Cl2, O3, SO3) was investigated by X-ray and potentiometric methods. It is shown that stage 2 (oxidizer, Cl2) and stage 1 (oxidizer, O3) are formed in 94% H2SO4. It was established that the rate of the stage 2 GHS formation depends on the Cl2 ultraviolet radiation, high pressure Cl2 (P = 40–70 atm) and temperature. As expected the rate of the stage 1 GHS formation (oxidizer, O3) was increased with content of O3 in a O3-O2 gaseous mixture. The graphite-oleum system was investigated in a wide range of oleum concentrations (5–57% of free SO3) by potentiometric and calorimetric methods. It was established that the potentials of GIC formation with oleum are different from potentials of GHS formation when salt-like, Cl2 or O3 are used as oxidizers. In addition, the heat flow curves have a monotonous behaviour. These factors were explained by the co-intercalation of SO3 with anions of sulphuric acid into graphite." @default.
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- W2469852445 date "1996-06-01" @default.
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- W2469852445 title "Investigation of the Graphite-H2SO4-gaseous oxidizer (Cl2, O3, SO3) system" @default.
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- W2469852445 doi "https://doi.org/10.1016/0022-3697(96)00359-9" @default.
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