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- W2469897711 abstract "A tert-butylcarbamoylquinine ( tBuCQUI)-incorporated silica hybrid monolithic (QUI–SHM) capillary was prepared by “one-pot” approach via simultaneous sol–gel reaction of tetramethoxysilane and vinyltrimethoxysilane and free radical polymerization of tBuCQUI. A set of acidic chiral drugs were enantioseparated on QUI–SHM in mobile phases consisting of acetonitrile (ACN), methanol (MeOH), acetic acid (AcOH), and triethylamine (TEA). Influences of ACN/MeOH ratio, AcOH/TEA ratio, and their concentrations on enantioseparation were investigated. Baseline separations of enantiomers of all the compounds investigated were achieved with a mobile phase of 60:38 (v/v) ACN/MeOH containing 350 mM AcOH and 30 mM TEA under the applied voltage of −10 kV at 25°C." @default.
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- W2469897711 date "2016-06-29" @default.
- W2469897711 modified "2023-09-24" @default.
- W2469897711 title "Enantiomer Separation of Acidic Chiral Compounds on a<i>tert</i>-Butylcarbamoylquinine-Silica Hybrid Monolith by Capillary Electrochromatography" @default.
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- W2469897711 doi "https://doi.org/10.1002/bkcs.10820" @default.
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