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- W2472637299 abstract "Abstract Two basic, previously unpublished procedures were developed to obtain flusilazole data for regula- tory purposes. One method involves extraction into ethyl acetate, cleanup on silica or Florisil, and analysis of flusilazole only by packed-column gas chromatography (GC) with nitrogen-phosphorus detection. The second method involves extraction into ethyl acetate, followed by gel permeation chro- matography and analysis by capillary GC with mass-selective detection for both IN-F7321 (major metabolite) and flusilazole. Several adaptations of the second procedure increase the analytical op- tions for flusilazole. The parent-only method was applied to analysis of more than 18 matrixes. The parent-plus-metabolite method and its adaptations were applied to the analysis of more than 33 ma- trixes. Cereals, fruits, animal matrixes and related processed fractions were analyzed. Average recov- eries for the parent-only method were generally above 90% (always above 80%) with standard devia- tions of 12% or less for fortifications ranging from 0.010 to 1.0 ppm. Average recoveries ranged from 84 to 108% for flusilazole and 82 to 111% for IN- F7321 fortifications from 0.010 to 2.0 ppm for the parent-plus-metabolite method. Standard devia- tions ranged from 3.6 to 20%." @default.
- W2472637299 created "2016-07-22" @default.
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- W2472637299 date "1994-05-01" @default.
- W2472637299 modified "2023-09-27" @default.
- W2472637299 title "Analysis of Flusilazole and Its Major Phenyl Metabolite (IN-F7321) by Approaches Based on Gas Chromatography" @default.
- W2472637299 doi "https://doi.org/10.1093/jaoac/77.3.728" @default.
- W2472637299 hasPublicationYear "1994" @default.
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