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- W2473750658 abstract "A method has been established to measure 9 perfluorinated compounds (PECs), including 2 perfluorinated sulfonates and 7 carboxylic acids (C7-C12, C14), in aquatic products (fish and shellfish). PFCs in fish and shellfish were extracted with a modified NaOH digestion WAX method, and the final eluate was reduced to I mL with nitrogen before injection. Under the optimal conditions, PFCs standards were recovered well through the whole pretreatment procedure with recoveries of 97.6%-120.8%. When applied to fish and shellfish samples, PFCs were also well recovered, except perfluorododecanoic acid (PFDoDA) and perfluorotetradexanoic acid (PFTA) for shellfish. With the use of high performance liquid chromatography/electrospray tandem mas spectrometry, 9 analysts were separated on Acclaim 120 C(18) reversed-phase column (150 mm X 4.6 mm, 5 mu m) in 10 min using CH(3)OH and 50 mmol/L NH(4)Ac gradient elution, and a detection limit of 0. 16 - 2. 0 ng/g for real samples analysis can he achieved." @default.
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- W2473750658 date "2008-12-01" @default.
- W2473750658 modified "2023-09-27" @default.
- W2473750658 title "Determination of 9 Perfluorinated Compounds in Aquatic Products: Fish and Shellfish" @default.
- W2473750658 hasPublicationYear "2008" @default.
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