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- W2474197822 abstract "Abstract An analytical method was developed to simultaneously determine sulfadimethoxine (SDM) and ormetoprim (OMP) in medicated animal feeds. SDM and OMP are extracted from the feed into methylene chloride at pH 10 following the addition of tetrabutylammonium hydroxide to form an ion pair with SDM. After the methylene chloride extract is dried over sodium sulfate, an aliquot is purified by solid-phase extraction using a PrepSep silica extraction column. Both compounds are separated by liquid chromatography on an Ultrasphere ionpair column at 3°0C with UV detection at 275 nm. The average recoveries for OMP and SDM in feeds fortified between 0.01 and 0.5% total combined drug ranged from 96.4 to 101.4%, respectively. Replicate assays of typical feeds yielded coefficients of variation of 1.7-3.1%." @default.
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- W2474197822 date "1993-03-01" @default.
- W2474197822 modified "2023-09-26" @default.
- W2474197822 title "Liquid Chromatographic Method for the Simultaneous Analysis of Sulfadimethoxine and Ormetoprim in Animal Feeds" @default.
- W2474197822 doi "https://doi.org/10.1093/jaoac/76.2.320" @default.
- W2474197822 hasPublicationYear "1993" @default.
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