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- W2476782663 abstract "The synthesis and handling of energetic materials requires several cautionary practices beyond what is normally expected for non-energetic compound processes. We describe herein the additional items that are taken into account as the synthesis and development of an energetic material progress. Topics addressed include what is an energetic material, sensitivity and stability measurements, synthetic design for safety, energy content determination and control methods, transportation, and waste disposal. Emphasis is placed on the use of differential scanning calorimetry, reaction calorimetry, and accelerating rate calorimetry to characterize the energetic-related hazards of a reaction and its products. The synthesis of 1-bromoacetyl-3,3-dinitroazetidine, a clinical anti-cancer candidate derived from the explosive 1,3,3-trinitroazetidine, is used as a model process for demonstrating some of the techniques described here." @default.
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- W2476782663 date "2014-01-01" @default.
- W2476782663 modified "2023-09-24" @default.
- W2476782663 title "Synthesis and Processing of Energetic Materials – Considerations for Safe Scale-up of Potentially Hazardous Reactions" @default.
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- W2476782663 doi "https://doi.org/10.1021/bk-2014-1181.ch010" @default.
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