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• W2479010031 startingPage "1244" @default.
• W2479010031 abstract "We report on the use of photoinitiated reversible addition-fragmentation chain transfer (RAFT) polymerization for the facile fabrication of cross-linked nanoporous polymer films with three-dimensionally (3D) continuous pore structure. The photoinitiated polymerization of isobornyl acrylate (IBA) in the presence of 2-(dodecylthiocarbonothioylthio)-2-methylpropionic acid (CTA) and 2,2-dimethoxy-2-phenylacetophenone as a photoinitiator proceeded in a controlled manner, yet more rapidly compared to thermally initiated polymerization. When polylactide-macroCTA (PLA-CTA) was used, PLA-b-PIBA with high molar mass was obtained after several minutes of irradiation at room temperature. We confirmed that microphase separation occurs in the PLA-b-PIBA and that nanoporous PIBA can be derived from the PLA-b-PIBA precursor by selective PLA etching. To fabricate the cross-linked nanoporous polymer, IBA was copolymerized with ethylene glycol diacrylate (EGDA) in the presence of PLA-CTA to produce a cross-linked block polymer precursor consisting of bicontinuous PLA and P(IBA-co-EGDA) microdomains, via polymerization-induced microphase separation. We demonstrated that nanoporous P(IBA-co-EGDA) monoliths and films with 3D continuous pores can be readily obtained via this approach." @default.
• W2479010031 created "2016-08-23" @default.
• W2479010031 creator A5004297961 @default.
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• W2479010031 date "2015-10-26" @default.
• W2479010031 modified "2023-09-25" @default.
• W2479010031 title "Photoinitiated Polymerization-Induced Microphase Separation for the Preparation of Nanoporous Polymer Films" @default.
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• W2479010031 doi "https://doi.org/10.1021/acsmacrolett.5b00734" @default.
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• W2479010031 hasPublicationYear "2015" @default.
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