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- W2480503199 abstract "The lithium enolates of O-ethyl S-(tetrahydro-2-oxo-3-furanyl) dithiocarbonate and thiocarbonate were found to be efficient reagents for the stereoselective synthesis of α-alkylidene-γ-butyrolactones from carbonyl compounds. The dianion of α-mercapto-γ-butyrolactone was successfully generated by treatment of α-mercapto-γ-butyrolactone with 2.2 equivalents of lithium diisopropylamide in the presence of N,N,N′,N′-tetramethylethylenediamine at −78°C in THF. The dianion thus formed has been utilized for the efficient and stereoselective synthesis of α-alkylidene-γ-butyrolactones from carbonyl compounds." @default.
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- W2480503199 date "1980-10-01" @default.
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- W2480503199 title "New Methods for Stereoselective Synthesis of α-Alkylidene-γ-butyrolactones Using Monoanion of<i>O</i>-Ethyl<i>S</i>-(Tetrahydro-2-oxo-3-furanyl) Thiocarbonate and Dianion of α-Mercapto-γ-butyrolactone" @default.
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- W2480503199 doi "https://doi.org/10.1246/bcsj.53.2910" @default.
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