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- W2484094041 abstract "Abstract Simple benzo‐fused nitrogen heterocycles (indolines, tetrahydroquinolines, and their homologues) undergo migratory ring expansion through deprotonation of their benzylic urea derivatives with lithium diisopropylamide (LDA) in the presence of N,N′‐dimethylpropylideneurea (DMPU). The products of the reactions are benzodiazepines, benzodiazocines, and their homologues, with ring sizes of 8–12. The reactions tolerate a range of substituent patterns and types, and may exhibit enantiospecificity or diastereoselectivity. Considerable complexity is rapidly generated in an efficient synthesis of these otherwise difficult‐to‐obtain medium‐ring nitrogen heterocycles." @default.
- W2484094041 created "2016-08-23" @default.
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- W2484094041 date "2016-07-21" @default.
- W2484094041 modified "2023-10-16" @default.
- W2484094041 title "Medium-Ring Nitrogen Heterocycles through Migratory Ring Expansion of Metalated Ureas" @default.
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- W2484094041 doi "https://doi.org/10.1002/anie.201605714" @default.
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