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- W2484687571 abstract "4′,4″(5″) Di-tert-butyldibenzo 18-crown-6 (DTBB18C6) was successfully synthesized by SN2 nucleophilic substitution with 4-tert-butyl catechol as starting material. Effects of cyclization reagents, solvents, and templates were investigated. Reaction process was monitored by the real-time online FTIR to study the actual reaction route. The highest DTBB18C6 yield (above 33%) was obtained by using Cs2CO3 as the template, 2,2′-diethylene glycol ditosylate as the cyclization reagent, and THF as the solvent. From the result of FTIR, four different reaction stages of DTBB18C6 synthesis process were proposed." @default.
- W2484687571 created "2016-08-23" @default.
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- W2484687571 date "2013-12-17" @default.
- W2484687571 modified "2023-09-26" @default.
- W2484687571 title "Synthesizing 4′,4″(5″) Di-tert-butyldibenzo 18-crown-6 Monitored by Online FTIR" @default.
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- W2484687571 doi "https://doi.org/10.1002/jhet.1815" @default.
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