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- W2484810071 abstract "In-situ electrochemical spectroscopic methods, such as solid-state nuclear magnetic resonance (NMR), attenuated-total-reflection surface-enhanced IR reflection adsorption spectroscopy (ATR-SEIRAS) and surface-enhanced Raman scattering spectroscopy (SERS), offer complementary atomic and molecular scale information on the electronic, structural, and molecular properties of nanoparticle electrocatalysts and mechanism(s) of surface reactions. In situ electrochemical (EC) 195Pt and 13CO NMR enables measurements of s- and d-like metal surface local density of states at the Fermi level (E f -LDOS) and 5σ- and 2π*-like E f -LDOS at the probing CO. Such quantitative, electronic-orbital-specific (EOS) information makes it possible to relate electronic properties of the electrocatalysts with surface reaction mechanism(s) that can be monitored by vibrational spectroscopy, i.e. ATR-SEIRAS and SERS. In this chapter, we discuss integrated in situ EC-NMR, -SEIRAS and -SERS studies of CO and methanol oxidation reactions on core-shell Ru@Pt and Au@Pt nanoparicles (NPs) through which we intend to demonstrate that the integrated approach makes “the whole is greater than the sum of its parts”." @default.
- W2484810071 created "2016-08-23" @default.
- W2484810071 creator A5007523718 @default.
- W2484810071 creator A5071054591 @default.
- W2484810071 creator A5091286949 @default.
- W2484810071 date "2016-01-01" @default.
- W2484810071 modified "2023-10-05" @default.
- W2484810071 title "Integrated Studies of Au@Pt and Ru@Pt Core-Shell Nanoparticles by In Situ Electrochemical NMR, ATR-SEIRAS, and SERS" @default.
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