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• W2484845481 abstract "The temperature dependence of the X-ray crystal structure and powder EPR spectrum of [(HC(Ph2PO)3)2Cu](ClO4)2·2H2O is reported, and the structure at room temperature confirms that reported previously. Below ∼100 K, the data imply a geometry with near elongated tetragonal symmetry for the [(HC(Ph2PO)3)2Cu]2+ complex, but on warming the two higher Cu−O bond lengths and g-values progressively converge, and by 340 K the bond lengths correspond to a compressed tetragonal geometry. The data may be interpreted satisfactorily assuming an equilibrium among the energy levels of a Cu−O6 polyhedron subjected to Jahn−Teller vibronic coupling and a lattice strain. However, agreement with the experiment is obtained only if the orthorhombic component of the lattice strain decreases to a negligible value as the temperature approaches 340 K." @default.
• W2484845481 created "2016-08-23" @default.
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• W2484845481 date "2005-03-17" @default.
• W2484845481 modified "2023-09-27" @default.
• W2484845481 title "Temperature Dependence of the Crystal Structure and <i>g</i>-Values of [(HC(Ph₂PO)₃)₂Cu](ClO₄)₂·2H₂O: Influence of Dynamic Jahn−Teller Coupling and Lattice Strain Interactions" @default.
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• W2484845481 doi "https://doi.org/10.1021/ic048604h" @default.
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